GLYCOSYL COMPOSITION ANALYSIS OF COLLAGEN SAMPLES

$1,221P41FY2000RRNIH

University Of Georgia (Uga), Athens GA

Investigators

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Abstract

For the FAB-MS analysis, all experiments were performed on a JEOL SX/SX102A tandem four-sector mass spectrometer operated at 10 kV accelerating potential. Ions were produced by fast atom bombardment with xenon using a JEOL FAB gun operated at 6 kV. The spectra were recorded in the positive ion mode with a resolution of approximately 1000 (90% valley). The spectra are averaged profile data of two scans as recorded by a JEOL complement data system. These spectra were acquired from 100 to 2500 m/z at a rate that would scan from m/z 100 to m/z 2500 in 1 minute with a filtering rate of 300 Hz.

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